Electropolymerized nanoporous polymeric SPME coatings: preparation and characterization by small angle X-ray scattering and scanning electron microscopy
Identifieur interne : 000090 ( Main/Exploration ); précédent : 000089; suivant : 000091Electropolymerized nanoporous polymeric SPME coatings: preparation and characterization by small angle X-ray scattering and scanning electron microscopy
Auteurs : Boguslaw Buszewski [Pologne] ; Pawel Olszowy [Pologne] ; Stanislaw Pikus [Pologne] ; Maciej Kozak [Pologne]Source :
- Monatshefte Fur Chemie [ 0026-9247 ] ; 2014.
Abstract
Polymeric polypyrrole and polythiophene solid phase microextraction (SPME) coatings were prepared using electropolymerization with a linear sweep voltammetry technique. Physicochemical properties were measured using different methods, in particular small angle X-ray scattering and scanning electron microscopy. By using innovative approaches for pore size measurement, we were able to calculate a maximum of the pore size range from 80 to 90 nm. Additionally, film thicknesses measured from 90 to 150 μm. Using scanning electron microscopy, we describe the characteristics of polymer growth on the support surface.
Url:
DOI: 10.1007/s00706-013-1115-3
PubMed: 26166891
PubMed Central: 4494846
Affiliations:
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Buszewski</name><affiliation wicri:level="1"><nlm:aff id="Aff1">Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun</wicri:regionArea></affiliation></author><author><name sortKey="Olszowy, Pawel" sort="Olszowy, Pawel" uniqKey="Olszowy P" first="Pawel" last="Olszowy">Pawel Olszowy</name><affiliation wicri:level="1"><nlm:aff id="Aff1">Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Environmental Chemistry and Bioanalytics, Faculty of Chemistry, Nicolaus Copernicus University, Gagarina 7, Torun</wicri:regionArea></affiliation></author><author><name sortKey="Pikus, Stanislaw" sort="Pikus, Stanislaw" uniqKey="Pikus S" first="Stanislaw" last="Pikus">Stanislaw Pikus</name><affiliation wicri:level="1"><nlm:aff id="Aff2">Department of Crystallography, Faculty of Chemistry, Maria Curie-Skłodowska University, Maria Curie-Skłodowska 3, 20-031 Lublin, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Crystallography, Faculty of Chemistry, Maria Curie-Skłodowska University, Maria Curie-Skłodowska 3, 20-031 Lublin</wicri:regionArea></affiliation></author><author><name sortKey="Kozak, Maciej" sort="Kozak, Maciej" uniqKey="Kozak M" first="Maciej" last="Kozak">Maciej Kozak</name><affiliation wicri:level="1"><nlm:aff id="Aff3">Department of Macromolecular Physics, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan, Poland</nlm:aff><country xml:lang="fr">Pologne</country><wicri:regionArea>Department of Macromolecular Physics, Faculty of Physics, Adam Mickiewicz University, Umultowska 85, 61-614 Poznan</wicri:regionArea></affiliation></author></analytic><series><title level="j">Monatshefte Fur Chemie</title><idno type="ISSN">0026-9247</idno><idno type="eISSN">1434-4475</idno><imprint><date when="2014">2014</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en"><sec><title>Abstract</title><p>Polymeric polypyrrole and polythiophene solid phase microextraction (SPME) coatings were prepared using electropolymerization with a linear sweep voltammetry technique. Physicochemical properties were measured using different methods, in particular small angle X-ray scattering and scanning electron microscopy. By using innovative approaches for pore size measurement, we were able to calculate a maximum of the pore size range from 80 to 90 nm. Additionally, film thicknesses measured from 90 to 150 μm. Using scanning electron microscopy, we describe the characteristics of polymer growth on the support surface.</p></sec><sec><title>Graphical abstract</title><p><graphic position="anchor" xlink:href="706_2013_1115_Figa_HTML" id="MO1"></graphic></p></sec></div></front><back><div1 type="bibliography"><listBibl><biblStruct><analytic><author><name sortKey="Janata, J" uniqKey="Janata J">J Janata</name></author><author><name sortKey="Josowicz, M" uniqKey="Josowicz M">M Josowicz</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Adhikari, B" uniqKey="Adhikari B">B Adhikari</name></author><author><name sortKey="Majumdar, S" uniqKey="Majumdar S">S Majumdar</name></author></analytic></biblStruct><biblStruct><analytic><author><name sortKey="Gerard, M" uniqKey="Gerard M">M Gerard</name></author><author><name sortKey="Chaubey, A" uniqKey="Chaubey A">A Chaubey</name></author><author><name sortKey="Malhotra, Bd" uniqKey="Malhotra B">BD 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sort="Buszewski, Boguslaw" uniqKey="Buszewski B" first="Boguslaw" last="Buszewski">Boguslaw Buszewski</name></noRegion><name sortKey="Kozak, Maciej" sort="Kozak, Maciej" uniqKey="Kozak M" first="Maciej" last="Kozak">Maciej Kozak</name><name sortKey="Olszowy, Pawel" sort="Olszowy, Pawel" uniqKey="Olszowy P" first="Pawel" last="Olszowy">Pawel Olszowy</name><name sortKey="Pikus, Stanislaw" sort="Pikus, Stanislaw" uniqKey="Pikus S" first="Stanislaw" last="Pikus">Stanislaw Pikus</name></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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